13 March 2024Measuring the nonlinear refraction as a function of depth in chemically tempered alkali-aluminosilicate glasses to infer the potassium concentration and mechanical strength
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We have determined the potassium penetration cross-section in chemically tempered glasses by nondestructive nonlinear refraction measurements. The nonlinear refraction as a function of the depth was measure by the Nonlinear Ellipse Rotation (NER) signal using ultrafast laser pulses (40 fs, 1 kHz, ~2000 GW/cm2 at 780 nm) from an amplified laser system. For local NER measurements, we have used a long distance objective (20x, 1.5 cm WD) which provides a relatively good penetration resolution (~5.5 microns). We characterized several glasses with different ion exchange treatment time. The potassium penetration depth and cross-section could be correlated with the materials’ hardness.
G. L. Santana,R. Barbosa,V. Tribuzi,F. G. Ghiglieno,E. D. Zanotto,P. H. D. Ferreira, andL. Misoguti
"Measuring the nonlinear refraction as a function of depth in chemically tempered alkali-aluminosilicate glasses to infer the potassium concentration and mechanical strength", Proc. SPIE 12878, High-Power Laser Materials Processing: Applications, Diagnostics, and Systems XIII, 128780M (13 March 2024); https://doi.org/10.1117/12.3002499
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G. L. Santana, R. Barbosa, V. Tribuzi, F. G. Ghiglieno, E. D. Zanotto, P. H. D. Ferreira, L. Misoguti, "Measuring the nonlinear refraction as a function of depth in chemically tempered alkali-aluminosilicate glasses to infer the potassium concentration and mechanical strength," Proc. SPIE 12878, High-Power Laser Materials Processing: Applications, Diagnostics, and Systems XIII, 128780M (13 March 2024); https://doi.org/10.1117/12.3002499